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- Title
Synthesis and Characterization of Organotin (IV) Dithiobiurets.
- Authors
Rastogi, R. B.; Singh, K.; Maurya, J. L.
- Abstract
Organotin complexes of the type Ph3SnL and Bu2SnL2 (where Ph = phenyl and Bu = butyl, HL = 1-phenyl-2, 4-dithiobiuret (PDTBH), 1-(3-acetylphenyl)-2, 4-dithiobiuret (AcPDTBH), 1-(4-ethoxyphenyl)-2, 4-dithiobiuret (EtOPDTBH)), have been prepared. Molar conductance studies show the nonionic behavior of the complexes. FAB mass spectra exhibit their monomeric nature. ¹H NMR and 13C NMR spectra of the complexes are consistent with the proposed stoichiometry of the complexes. Infrared spectra indicate anionic bidentate coordinating behavior of the ligands. Powder X-ray diffraction patterns of the complex Ph3Sn (PDTB) are indicative of monoclinic system.
- Publication
IUP Journal of Chemistry, 2011, Vol 4, Issue 3, p7
- ISSN
0974-6552
- Publication type
Academic Journal